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[{"key": "dc.contributor.advisor", "value": "Matilainen, Rose", "language": "", "element": "contributor", "qualifier": "advisor", "schema": "dc"}, {"key": "dc.contributor.author", "value": "Kylm\u00e4l\u00e4, Tiina", "language": "", "element": "contributor", "qualifier": "author", "schema": "dc"}, {"key": "dc.date.accessioned", "value": "2024-08-12T06:45:47Z", "language": null, "element": "date", "qualifier": "accessioned", "schema": "dc"}, {"key": "dc.date.available", "value": "2024-08-12T06:45:47Z", "language": null, "element": "date", "qualifier": "available", "schema": "dc"}, {"key": "dc.date.issued", "value": "2024", "language": "", "element": "date", "qualifier": "issued", "schema": "dc"}, {"key": "dc.identifier.uri", "value": "https://jyx.jyu.fi/handle/123456789/96562", "language": null, "element": "identifier", "qualifier": "uri", "schema": "dc"}, {"key": "dc.description.abstract", "value": "T\u00e4m\u00e4n pro gradu -tutkielman kirjallisessa osassa perehdyt\u00e4\u00e4n syv\u00e4llisesti ICP-OES-laitteistoon sek\u00e4 sen mittausmenetelmien kehitykseen. ICP-OES-laitteiston n\u00e4ytteensy\u00f6t\u00f6n ja spektrometrin osat esitell\u00e4\u00e4n ja pohditaan niiden vaikutuksia analyysiin. Kirjallisessa osassa k\u00e4sitell\u00e4\u00e4n my\u00f6s ICP-OES-laitteiston menetelm\u00e4kehityksen vaiheita ja arviointia.\n\nKirjallisessa osassa kerrotaan kuningasvesiuutosta sek\u00e4 muista mahdollisista uuttotekniikoista. Pro gradu -tutkielma on tehty Eurofins Labtiumin laboratoriossa, joka on FINAS akkreditoitu laboratorio. Kirjallisuus osioissa k\u00e4yd\u00e4\u00e4n l\u00e4pi, miten akkreditointivaatimukset vaikutavat kokeellisen osion suorittamiseen. Validointiparametrej\u00e4 ja niiden laskukaavoja k\u00e4yd\u00e4\u00e4n my\u00f6s l\u00e4pi kirjallisessa osiossa.\n\nKokeellisessa osiossa pyrittiin kehitt\u00e4m\u00e4\u00e4n ICP-OES-laitteistolle mittausmenetelm\u00e4, jolla pystytt\u00e4isiin analysoimaan kuningasvesiuuttoliuoksista toistettavasti ja luotettavasti 32 alkuainetta, v\u00e4hint\u00e4\u00e4n laboratorion aieimpien mittausmenetelmien mukaisesti. Ty\u00f6ss\u00e4 etsittiin parhaimmat aallonpituudet mitattaville alkuaineille, etsittiin niille matriisin mukaan parhaimmat taustankorjauspaikat ja tarkastettiin interelemettikertoimien tarpeellisuus. Kun menetelm\u00e4 saatiin kehitetty\u00e4 laitteelle, aloitettiin analyysitulosten mittausten tekeminen validointia varten.\n\nValidointi suoritettiin sertifioitujen referenssimateriaalien, reagenssinollien sek\u00e4 duplikaatti n\u00e4ytteiden avulla. Validoinnissa tarkastettiin m\u00e4\u00e4ritysraja, spesifisyys, lineaarisuus, herkkyys, toistettavuus, uusittavuus, oikeellisuus sek\u00e4 mittausep\u00e4varmuus. Validoinnista saatujen tulosten perusteella kehitetylle mittausmenetelm\u00e4lle voidaan hakea laajempaa akkreditointia seuraavassa FINAS-auditoinnissa.", "language": "fi", "element": "description", "qualifier": "abstract", "schema": "dc"}, {"key": "dc.description.provenance", "value": "Submitted by Miia Hakanen (mihakane@jyu.fi) on 2024-08-12T06:45:47Z\nNo. of bitstreams: 0", "language": "en", "element": "description", "qualifier": "provenance", "schema": "dc"}, {"key": "dc.description.provenance", "value": "Made available in DSpace on 2024-08-12T06:45:47Z (GMT). No. of bitstreams: 0\n Previous issue date: 2024", "language": "en", "element": "description", "qualifier": "provenance", "schema": "dc"}, {"key": "dc.format.extent", "value": "105", "language": "", "element": "format", "qualifier": "extent", "schema": "dc"}, {"key": "dc.language.iso", "value": "fin", "language": null, "element": "language", "qualifier": "iso", "schema": "dc"}, {"key": "dc.rights", "value": "In Copyright", "language": "en", "element": "rights", "qualifier": null, "schema": "dc"}, {"key": "dc.subject.other", "value": "ICP-OES", "language": "", "element": "subject", "qualifier": "other", "schema": "dc"}, {"key": "dc.subject.other", "value": "monimetalli", "language": "", "element": "subject", "qualifier": "other", "schema": "dc"}, {"key": "dc.title", "value": "ICP-OES-Duolaitteiston k\u00e4ytt\u00f6\u00f6notto ja kuningasvesi-uuttoliuosten mittausmenetelm\u00e4n validointi akkreditoidussa laboratoriossa", "language": "", "element": "title", "qualifier": null, "schema": "dc"}, {"key": "dc.type", "value": "master thesis", "language": null, "element": "type", "qualifier": null, "schema": "dc"}, {"key": "dc.identifier.urn", "value": "URN:NBN:fi:jyu-202408125438", "language": null, "element": "identifier", "qualifier": "urn", "schema": "dc"}, {"key": "dc.type.ontasot", "value": "Master\u2019s thesis", "language": "en", "element": "type", "qualifier": "ontasot", "schema": "dc"}, {"key": "dc.type.ontasot", "value": "Pro gradu -tutkielma", "language": "fi", "element": "type", "qualifier": "ontasot", "schema": "dc"}, {"key": "dc.contributor.faculty", "value": "Matemaattis-luonnontieteellinen tiedekunta", "language": "fi", "element": "contributor", "qualifier": "faculty", "schema": "dc"}, {"key": "dc.contributor.faculty", "value": "Faculty of Sciences", "language": "en", "element": "contributor", "qualifier": "faculty", "schema": "dc"}, {"key": "dc.contributor.department", "value": "Kemian laitos", "language": "fi", "element": "contributor", "qualifier": "department", "schema": "dc"}, {"key": "dc.contributor.department", "value": "Department of Chemistry", "language": "en", "element": "contributor", "qualifier": "department", "schema": "dc"}, {"key": "dc.contributor.organization", "value": "Jyv\u00e4skyl\u00e4n yliopisto", "language": "fi", "element": "contributor", "qualifier": "organization", "schema": "dc"}, {"key": "dc.contributor.organization", "value": "University of Jyv\u00e4skyl\u00e4", "language": "en", "element": "contributor", "qualifier": "organization", "schema": "dc"}, {"key": "dc.subject.discipline", "value": "Analyyttinen kemia", "language": "fi", "element": "subject", "qualifier": "discipline", "schema": "dc"}, {"key": "dc.subject.discipline", "value": "Analytical Chemistry", "language": "en", "element": "subject", "qualifier": "discipline", "schema": "dc"}, {"key": "yvv.contractresearch.collaborator", "value": "business", "language": "", "element": "contractresearch", "qualifier": "collaborator", "schema": "yvv"}, {"key": "yvv.contractresearch.funding", "value": "0", "language": "", "element": "contractresearch", "qualifier": "funding", "schema": "yvv"}, {"key": "yvv.contractresearch.initiative", "value": "business", "language": "", "element": "contractresearch", "qualifier": "initiative", "schema": "yvv"}, {"key": "dc.type.coar", "value": "http://purl.org/coar/resource_type/c_bdcc", "language": null, "element": "type", "qualifier": "coar", "schema": "dc"}, {"key": "dc.rights.accesslevel", "value": "openAccess", "language": null, "element": "rights", "qualifier": "accesslevel", "schema": "dc"}, {"key": "dc.type.publication", "value": "masterThesis", "language": null, "element": "type", "qualifier": "publication", "schema": "dc"}, {"key": "dc.subject.oppiainekoodi", "value": "40311", "language": "", "element": "subject", "qualifier": "oppiainekoodi", "schema": "dc"}, {"key": "dc.subject.yso", "value": "kuningasvesi", "language": null, "element": "subject", "qualifier": "yso", "schema": "dc"}, {"key": "dc.subject.yso", "value": "validointi", "language": null, "element": "subject", "qualifier": "yso", "schema": "dc"}, {"key": "dc.subject.yso", "value": "analyysi", "language": null, "element": "subject", "qualifier": "yso", "schema": "dc"}, {"key": "dc.subject.yso", "value": "laatu", "language": null, "element": "subject", "qualifier": "yso", "schema": "dc"}, {"key": "dc.rights.url", "value": "https://rightsstatements.org/page/InC/1.0/", "language": null, "element": "rights", "qualifier": "url", "schema": "dc"}]
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